This manual represents laboratory practicums and individual tasks in the main areas of physical chemistry, which determine its subject matter: chemical thermodynamics, chemical equilibrium, phase equilibriums and the theory of solutions, kinetics and catalysis, and solutions of electrolytes. The present teaching materials are addressed to undergraduate and graduate students majoring in chemical engineering, who study «Physical Chemistry» and «Supplementary Materials of Physical Chemistry» as academic disciplines. Developed at the Department of Physical and Colloid Chemistry.